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GCMS analysis results, sample AE12151, June 2002

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Gas chromatography-mass spectrometry analysis report for sample AE12151, completed on 6/6/02 at 14:58, testing for unknown compounds and 2,4-DDD surrogate.

NYC-WTC_000014902–000014911

Folder label: “GCMS X 5/29/02 A 5/31/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\MAY3102\12151.D Vial: 8 Acq On : 31 May 2002 6:52 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 3 9:29 2002 Quant Results File:rGCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.49 178 302 N.D. 36) Di-n-butylphthalate 27.41 149 5081 N.D. 37) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.48 228 2313 N.D. 42) Bis(2-ethylhexyl)phthalate 33.72 149 1573 N.D. 43) Chrysene 33.48 228 2313 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 4 6) Benzo(b)fluoranthene 36.52 252 324 N.D. 47) Benzo(k)fluoranthene 36.59 252 221 N.D. 48) Benzo(a)pyrene 37.67 252 2547 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 12151.D GCMS0531.M Mon Jun 03 09:29:56 2002 Page 2

NYC-WTC_000014905

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NYC-WTC_000014905Source: NYC Law Department, mirrored locally

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