GCMS calibration data AE12095, DEP Labs, May 2002

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Calibration table and internal standard data for sample AE12095 analyzed on May 31, 2002.

NYC-WTC_000014825–000014835

Folder label: “GCMS X 5/29/02 A 5/30/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY3 002\12096.D Vial: 15 Acq On : 31 May 2002 3:50 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 11:27 2002 Quant Results File:GCMS0520.RES Quant Method : C:\PCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0528

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.07 152 557022 40.00 ug/1 -0.07 10) Naphthalene-d8 15.70 136 2250799 40.00 ug/1 -0.10 17) Acenaphthene-diO 20.99 164 1065313 40.00 ug/1 -0.10 30) Phenanthrene-diO 25.43 188 1648656 40.00 ug/1 -0.11 38) Chrysene-dl2 33.47 240 991731 40.00 ug/1 -0.14 44) Perylene-dl2 37.66 264 628102 40.00 ug/1 -0.15

System Monitoring Compounds 28) TCMX 23.13 209 187886 35.09 ug/L -0.10 Spiked Amount 40.000 Recovery 87.73% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.44 74 394 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.05 146 225 N.D. 5) 1,4-Dichlorobenzene 12.05 146 225 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.76 128 224 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.48 149 5571 N.D. 26) 4-Chlorophenylphenylether 23.13 204 1264 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.43 178 579 N.D. (#) = qualifier out of range (m) = manual integration 12096.D GCMS0520.M Fri May 31 11:27:20 2002 Page 1

NYC-WTC_000014827

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