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GCMS analysis results for sample AE12538, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12538 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014660–000014669

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\JUNO 302\12538.D Vial: 19 Acq On 4 Jun 2002 2:57 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.068 326 329 342 rBV 25333 67894 1.99% 0.370% 2 12.062 759 764 785 rBV 931386 2421307 70.89% 13.201% 3 15.697 1154 1160 1176 rBV 1518612 3300653 96.64% 17.995% 4 20.985 1730 1736 1757 rBV 1545997 3389457 99.24% 18.479% 5 23.133 1962 1970 1978 rBV 814652 1687685 49.41% 9.201% 6 25.428 2213 2220 2231 rBV2 1570057 3415424 100.00% 18.621% 7 25.566 2231 2235 2251 rVB2 12916 47127 1.38% 0.257% 8 33.470 3090 3096 3112 rBV2 1021454 2377288 69.60% 12.961% 9 37.647 3544 3551 3562 rBV2 555990 1635278 47.88% 8.915%

Sum of corrected areas: 18342113 12538.D GCMS0531.M Tue Jun 04 11:52:05 2002

NYC-WTC_000014665

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NYC-WTC_000014665Source: NYC Law Department, mirrored locally

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