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GCMS surrogate recovery results, sample AE12535, June 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE12535 including surrogate recovery data on June 7, 2002.

NYC-WTC_000014632–000014640

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\JUNO 302\12535.D Vial: 16 Acq On ‘ 3 Jun 2002 11:59 pm Operator: Sample gc/ms scan 5/28 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R. T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.068 326 329 339 rBV 24917 63611 1.79% 0.337% 2 12.071 759 765 780 rBV 976253 2552823 72.01% 13.522% 3 15.697 1154 1160 1178 rBV 1579813 3444733 97.17% 18.246% 4 20.994 1730 1737 1754 rBV 1655687 3512385 99.08% 18.605% 5 23.133 1961 1970 1980 rBV 859056 1745491 49.24% 9.246%

6 25.428 2213 2220 2232 rBV2 1652205 3545040 100.00% 18.778% 7 33.470 3088 3096 3113 rBV2 1033437 2398310 67.65% 12.703% 8 37.647 3544 3551 3569 rBV2 542971 1616786 45.61% 8.564%

Sum of corrected areas: 18879179 12535.D GCMS0531.M Tue Jun 04 11:51:28 2002

NYC-WTC_000014637

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NYC-WTC_000014637Source: NYC Law Department, mirrored locally

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