NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\052902\12478.D Vial: 20
Acq On : 30 May 2002 1:34 am Operator: McLean
Sample : gc/ms scan 5/28 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 1 Butanoic acid, methyl ester Concentration Rank 16
R.T. EstConc Area Relative to ISTD R.T.
3.47 0.21 ug/L 150926 1,4-Dichlorobenzene-d4 9.90
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 9
2 Phosphonic dichloride, (2,2-dime... 188 C5H11C12OP 054552-71-5 9
3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 9
4 Butanoic acid, methyl ester 102 C5H10O2' 000623-42-7 9
Abundance Scan 67 (3.473 min): 12478.D (-62) (-) m/z 43.10 100.00%
43
5000
UZI
51 1
59
74
88 WN
. । . . -r-i-[-T-r-r-r-]~r-r
3.20 3.40 3.60 3.80
A
01 1+ ‘ i “ “ i ‘ • ■ i ■11 i ■ ■1 • i ■ " ■ f ■ ‘ “ i ■ “ • i ■ “ ■ i ■' “ i ■ “ ■ i • ‘ “ i m/ z 74.10 72.41%
niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160
Abundance #109994: Butanoic acid, methyl ester
43
74
5000 I** t—r-[—r-r-r-r
27 3.20 3.40 3.60 3.80
15 59 m/z 72.12%
1
87
miz->
01TImgu 1# + 102
•T“"!+ TIadtmua0u*mummTanOuTr
10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160
Abundance #24356: Phosphonic dichloride, (2,2-dimethylpropy!)-
43 71
320 3.40 3.60 3.80
5000 m/z 41.05 32.55%
vbuNw
27
55
m/z->
Ot 12" —354 I, rrtet
| . . 63 i, 83
’ha । n rl" i ri । I'd 11
101 117
* r1-1" । >11"*t
160
TTPmTTTTHT
10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160
Abundance #28312:3,3-Dichloropropyne ' ■ i ■ ■ • • i ■ • • ■ i 1 ■ ■ ' i • • ■ ■
74 3.20 3.40 3,60 3.80
MwuGM"*
m/z 87.95 32.55%
5000:
38
47
60 82 108
0 TTT — '■ i1 ■1 ■ i ■ ■ “ i ‘ ■11" ■ ■ i “ “ i •" • i11' ■ i ■ ■ i ■ “ ■ i
m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 3.20 3.40 3,60 3.80
12478.D 052202.M Mon Jun 03 11:40:25 2002 Page 4
NYC-WTC_000014468
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