GCMS analysis results, sample AE12322, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052902\12322.D vial: 10 Acq On : 29 May 2002 5:25 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan 15 Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.54 0.28 ug/L 178982 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 43 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 32 3 Allyl mercaptan 74 C3H6S 000870-23-5/9 4 Propanoic acid 74 C3H602 000079-094 5 Abundance Scan 78 (3.538 min): 12322.D (-74) (-) m/z 74.00 100.00% 74

5000

ol ■ 1 1 1 1 ■ ■ 1 1 1 1 1 1 1 1 35 49

11292.10,155 60 70 ...... I ■ i ■ ■ ■ ■ i ■ ‘lid 82

' i ■ ' ■ ■ i ■ ■ ■ ■ i ■ ' 1 ■ i . w, 3 20 m/z 3.40 82.00 3.60 3.80 60.00% *—T

w miz-> 10 20 30 40 50 80 90 100 110 Abundance #28338: Acetonitrite, dichloro- 74

5000 82 MAuCnoMual 47 3.20 3.40 3.60 3.80 35 m/z 76.00 39.54%

m/z-> Of 12 26 | 1 1 1 1 ' 1 1 ' ! 1 i'l ' | ■ । i I । । -2—1 ,1 ■ i ■ ■ ■ ■ i ■ • 108 ■ 1 I • ■ ■ ■ i

10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 3.20 . .Mi. . 3.40 3.60 3.80 5000 82 m/z 49.10 .30.99% 47

ol ■ ■ i ' ■ ■ '"i 1 1 1 1 i 1 1 1 11d ■ ■ i ■ ■ ■ • i ■ 1 • i • ■ ■ • i ■ ■ ■ ■ i ‘ ■ i miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161: Allyl mercaptan ' i * * • ■ i ■ * * * i • ■ * ' i ' 1 ■ ■ i 41 74 3.20 3.40 3.60 3.80 m/z 47.10 27.90% 50001

47 La//tu 27 33 i . 1,53.^ . ■ ■%! 0 1 ' i ‘ ‘ ■ i ‘ • i ■ ■ ■ ■ i ' ‘ ‘ i ■ i ■ ' ■ ■ i • ' 1 • i • ■ • • 1 1 ■ ■ 1 i Wz-> 10 20 30 401 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80

12322.D 052202.M Mon Jun 03 10:49:32 2002 Page 4

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