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GCMS analysis results for sample AE11602, June 2002

Machine-extracted title · confidence 90%

TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.

NYC-WTC_000013943–000013967

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary Operator ID: Date Acquired: 22 May 2002 8:06 pm Data File: C:\HPCHEM\l\DATA\MAY2102\11602.D Name: EXTRACTS/20 Mise: 2** Method: C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) e- Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Methyl Isobutyl /Keto 5.68 2.7 ug/1 173305 ISTD01 12.15 2567100 40.0 2-Pentanone, 4 -hydro 8.11 18.0 ug/1 1154880 ISTD01 12.15 2567100 40.0 Benzene, 1,2- .methy 8.82 0.5 ug/1 33348 ISTD01 12.15 2567100 40.0 p-Xylene 9.41 0.5 ug/1 34189 ISTD01 12.15 2567100 40.0 Cyclopentane/ 1,1-di 10.31 0.5 ug/1 31951 ISTD01 12.15 2567100 40.0 1-Octene, 3 ethyl- 10.35 0.9 ug/1 56412 ISTD01 12.15 2567100 40.0 Furan, 2,3 -dihydro - 10.52 0.7 ug/1 45967 ISTD01 12.15 2567100 40.0 Acetic acid, hexyl e 12.03 0.5 ug/1 32605 ISTDOl 12.15 2567100 40.0 Acetic acid, decyl e 12.72 0.5 ug/1 31556 ISTDOl 12.15 2567100 40.0 1-Pentanol, 2-methyl 12.98 1.8 ug/1 117915 ISTDOl 12.15 2567100 40.0 Acetic acid, hexyl e 13.11 2.0 ug/1 126541 ISTDOl 12.15 2567100 40.0 Acetic acid, 2-ethyl 13.15 4.0 ug/1 258852 ISTDOl 12.15 2567100 40.0 1-Hexanal, 5-methyl- 13.25 7.9 ug/1 5063'36 ISTDOl 12.15 2567100 40.0 Cyc lopepit ane, 1,3-di 13.35 6.9 ug/1 442738 ISTDOl 12.15 2567100 40.0 2-Propanoic acid, 2- 13.40 2.4 ug/1 151356 ISTDOl 12.15 2567100 40.0 1-Hexanol, 4-methyl- 13.51 8.6 ug/1 548916 ISTDOl 12.15 2567100 40.0 Acetic acid, heptyl 14.09 2.3 ug/1 183474 ISTD02 15.77 3150050 40.0 1-Decanol 14.27 1.1 ug/1 87397 ISTD02 15.77 3150050 40.0 Pentane, 3-methyl- 14.35 1.2 ug/1 94353 ISTD02 15.77 3150050 40.0

11602.D GCMS0520.M Fri May 24 08:33:21 2002

NYC-WTC_000013967

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NYC-WTC_000013967Source: NYC Law Department, mirrored locally

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