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GCMS calculation results for sample AE11602, May 2002

Machine-extracted title · confidence 90%

GCMS analysis report for sample AE11602 dated June 4, 2002, documenting unknown compounds and surrogate recovery.

NYC-WTC_000013921–000013942

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\052802\11602.D Vial: 8 Acq On : 28 May 2002 8:00 pm Operator: McLean Sample : 5/24 ad re-ext Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.226 22 25 33 W 6 4358 63554 0.16% 0.028% 2 3.379 50 51 74 PV 9 2309 72160 0.18% 0.032% 3 3.538 74 78 91 PV 6 5777 121477 0.30% 0.054% 4 3.720 91 109 117 PV 5 44295 2611019 6.50% 1.170% 5 3.779 117 119 121 W 3 37674 502869 1.25% 0.225% 6 3.796 121 122 124 W 2 35371 382715 0.95% 0.172% 7 3.820 124 126 138 W 5 32106 1364251 3.40% 0.611% 8 3.896 138 139 141 W 2 21351 242790 0.60% 0.109% 9 3.920 141 143 146 W 3 19360 265642 0.66% 0.119% 10 3.943 146 147 152 W 4 15651 328015 0.82% 0.147%

11 3.984 152 154 167 W 8 11641 284375 0.71% 0.127% 12 4.842 295 300 302 PV 5 2718 23679 0.06% 0.011% 13 5.018 326 330 333 W 4 3166 45639 0.11% 0.020% 14 5.048 333 335 343 W 7 3951 87567 0.22% 0.039% 15 5.177 355 357 367 PV 9 1998 68698 0.17% 0.031% 16 5.341 381 385 386 W 3 2808 32542 0.08% 0.015% 17 5.365 386 389 407 W 8 3961 159542 0.40% 0.072% 18 5.482 407 409 412 PV 3 2171 19546 0.05% 0.009% 19 5.929 478 485 509 PV 372452 8108474 20.20% 3.634% 20 6.334 552 554 559 PV 6 1919 25537 0.06% 0.011%

21 7.709 784 788 794 PV 5 4190 69408 0.17% 0.031% 22 8.790 967 972 976 PV 5 2638 50880 0.13% 0.023% 23 9.895 1152 1160 1180 W 1299396 26251635 65.39% 11.765% 24 10.224 1212 1216 1221 PV 5 2013 35940 0.09% 0.016% 25 11.998 1514 1518 1523 PV 5 1955 31869 0.08% 0.014% 26 12.375 1576 1582 1589 W 24244 370974 0.92% 0.166% 27 13.391 1739 1755 1776 PV 1955714 35391023 88.16% 15.862% 28 13.544 1776 1781 1789 W 5060 90305 0.22% 0.040% 29 15.659 2137 2141 2147 W 4 2006 31934 0.08% 0.014% 30 16.705 2311 2319 2332 PV 5 3128 69542 0.17% 0.031% 31 17.110 2383 2388 2395 W 3 7084 111602 0.28% 0.050% 32 17.621 2465 2475 2482 PV 5 2836 49242 0.12% 0.022% 33 18.526 2619 2629 2645 PV 2076652 39564844 98.55% 17.732% 34 20.101 2893 2897 2903 W 3 1717 28549 0.07% 0.013% 35 20.506 2951 2966 2979 BV 1152360 22249241 55.42% 9.972% 36 21.352 3105 3110 3116 W 2 10152 146118 0.36% 0.065% 37 22.533 3300 3311 3319 W 3 13703 257768 0.64% 0.116% 11602.D 052202.M Thu May 30 10:38:01 2002 Page 1

NYC-WTC_000013926

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NYC-WTC_000013926Source: NYC Law Department, mirrored locally

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