GCMS data file header for May 24-28, 2002

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Data File : C:\MSDCHEM\l\DATA\052802\524LB.D Vial: 3 Acq On : 28 May 2002 3:56 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 30 10:43:44 2002 Quant Results File: 052202.RES g** Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 29 08:47:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9,89 152 4468323 40.00 ug/L -0.01 10) Napthalene-d8 13.39 136 17694333 40.00 ug/L -0.02 17) Acenapthalene-dlO 18.53 164 9633664 40.00 ug/L -0.01 29) Phenanthranene-dlO 22.91 188 14601266 40.00 ug/L -0.01 37) Chrysene-dl2 30.76 240 10182671 40.00 ug/L -0.05 43) Perylene-dl2 34.65 264 5778544 40.00 ug/L -0.03

System Monitoring Compounds 27) TCMX 20.50 209 2147242 38.68 ug/L -0.01 Spiked Amount 40.000 Recovery 96.70% Target Compounds Qvalue 2) n-nitros-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Di chiorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichiorobenzene 0.00 146 0 N.D. 7) 2,2'oxybis(1-Chloropropane 0.00 45 0 N.D. 8) N-nitroso-di-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 13.39 93 -1813 Below Cal # l 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Napthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) 2-Chloronaphthalene 0,00 162 0 N.D. 19) Dimethylphthalate 0.00 163 0 N.D. 20) 2,6-Dinitrotoluene 0.00 165 0 N.D. 21) Acenapthylene 0.00 152 0 N.D. 22) Acenapthalene 0.00 153 0 N.D. 23) 2,4-Dinitrotoluene 0.00 165 0 N.D. 24) Diethylphthalate 0.00 149 0 N.D. 25) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 26) Fluorene 0.00 166 0 N.D. 28) Azobenzene 20.50 77 35430 N.D. 30) Nnitrosodiphenylamine 20.50 169 39816 0.27 ug/L # 57 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. . 35) Di-n-butylphthalate 25.04 149 46139 N.D. (#) = qualifier out of range (m) = manual integration 524LB.D 052202.M Thu May 30 10:43:55 2002 Page 1

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