GCMS analysis results for sample AE11928, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11928.D Vial: 8 Acq On : 23 May 2002 3:40 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 3-Furanmethanol Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.19 0.96 ug/L 703302 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua 1 3-Furanmethanol 98 C5H602 004412-91-3 9 2 Methylene Chloride 84 CH2C12 000075-09-2/9 3 Piperidine, 3-dimethylamino-l-me... 142 C8H18N2 1000126-80/8 9 4 Benzen-d5-amine 98 C6H2D5N 004165-61/1 9 Abundance Scan 190 (4.196 min): 11928.D (-186) (-) m/z 49.10 100.00% 49 98

5000 42 58 70 85 3.80 4.00 4.20 4.40 4.60 O' TITT ’ 14**14* -11’1’111/11213212111153311 m/z 98.10 88.78% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #42476:3-Furanmethanol 98

5000 41 69 81 ..... Il..... 3.80 4.00 4.20 4.40 4.60 53 m/z 51.10 36.51% 29

niz-> O+ ' 1 i 1 10 15 1 i 1 20 +4+ 40 50 60 70I80H 30 T+ 90 1(X) 110 120 130 140 'l ■ ■ ■ ■ i ■ ■ ' ■ i ■ ■ ■ ‘ i 1 1 ■ 1 i ■ ■ ■ ' i

Abundance #111040: Methylene Chloride 49 84 3.80 4.00 4.20 4.40 4.60 5000 m/z 100.20 31.82% 35

01 —14.28.42.1 10 20 30 40 70 ■ i •'1 • 11 ■ " i ■ 50 60 70 80 90 100 110 120 130 140 Abundance #42663: Piperidine, 3-dimethylamino-1-methyl- ■ i ■ ■ ■ ' i ' 1 ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ 98 3.80 4.00 4.20 4.40 4.60 m/z 58.10 30.26%

5000]

70 42 82 m/z—> 0 'I ■■■ ryssssglmopi 55 62 , । 110 1*t —Hr ThTT. 127 142 10 20 30 40 50 60 70 80 90 100 110 120 130 140 3.80 4.00 4.20 4.40 4.60

11928.D 052202.M Wed May 29 09:48:47 2002 Page 10

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