Laboratory report showing blank sample analysis for volatile organic compounds using gas chromatography-mass spectrometry on May 22, 2002.
NYC-WTC_000013049–000013076Folder label: “GCMS X 5/21/02 A 5/21/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\052102\LB.D Vial: 10 Acq On 21 May 2002 8:40 pm Operator: Mclean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 Cyclononasiloxane, octadeca... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 35.38 1.46 ug/L 1136330 Perylene-dl2 34.67 Hit# of 5 Tentative ID MW MolForm CAS#
1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 38 4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35 Abundance Scan 5497 (35.377 min): LB.D (-5487) (-) m/ z 73.05 1 .00% 73 147 221
5000 281 355 ‘ r l‘ 1 429 3500 35.20 35.40 35.60 35.80
miz-> 0- 44 ■ ‘ 11 ■ 1-‘ i ■1 - 191 13254 —fr ... .......... 503................................. 50 100 150 200 250 300 350 400) 450 500 550 600 .650 m/z 147.10 77.46% Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429
. i ■1. 355 5000 281 3500 35.20 35.40 35.60 35.80 m/z 221.10 75.02% 475 651 0- ' ■11 ’ ■ ■ ■ i • ■ 1...... 4/... M — miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 221 ....... R......... 73 3500 35.20 35.40 35.60 35.80 5000 m/z 281.00 38.09% 191 279 28 . 0- TTt — 2501................. miz-> 50 100 150 200 250 ‘360' '356' 400 450 500 550 600 650 Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 35.00 35.20 35.40 35.60 35.80 147 m/z 355.10 29.78% 5000 281 369
/z-> 0 L 50 100 117 150 207 249 200 250 300 350 400 450 500 550 600 650 ___________ 35.00 35.20 35.40 35.60 35.80
LB.D 052202.M Wed May 22 12:03:25 2002 Page 2 0
NYC-WTC_000013072
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NYC-WTC_000015496
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on June 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013285
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013154
GCMS laboratory report for sample AE09677 detecting unknown compounds and 2,4-DDD on May 23, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012751
Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015224
Laboratory report documenting GCMS analysis of sample AE12736 with surrogate recovery data and identification of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043893
Laboratory report for sample AE09771 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000013043
DEP document containing gas chromatography-mass spectrometry data from May 2002.
Filed in the same folder
NYC-WTC_000013044
Fragmented header page from a GCMS document batch dated May 2002 showing Method 508.
Filed in the same folder
NYC-WTC_000013077
Laboratory report showing calibration analysis for volatile organic compounds using gas chromatography-mass spectrometry on May 22, 2002.
Filed in the same folder
NYC-WTC_000013081
Reference standard analysis data for gas chromatography-mass spectrometry testing of volatile organic compounds on May 22, 2002.
Filed in the same folder
NYC-WTC_000013089
GCMS laboratory report for sample AE09517 detecting unknown compounds and 2,4-DDD on May 23, 2002.
Filed in the same folder