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GCMS sample analysis results, AE11903, June 3, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.

NYC-WTC_000012908–000012936

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11903.D Vial: 10 Acq On : 22 May 2002 9:09 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ** Library- : C:\DATABASE\NIST98.L ************ * * ******************************************************* Peak Number 16 Cyclononasiloxane, octadeca... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. • 34.32 1.59 ug/L 903195 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 64 2 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 38 3 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 37 4 2,6-Dimethyl-3,4-bis(trimethylsi... 311 C15H29NO2Si2 1000079-52-1 32 Abundance Scan 5318 (34.326 min): 11903.D (-5308) (-) m/z 73.10 •00.00% 73 147 221 5000 281 355 429 TTIfir TtrTi 34.00 34.20 34.40 34.60 nah 11325 40 . 191 , [ 503 0- 1 * * ■' 1 • 1’ । • —r 'i " 11111 ?i ----- m/z 147.10 66.40% m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429

355 5000 281 34.00 34.20 34.40 34.60 m/z 221.10 60.52% 475 I • i • ■ ■' i‘ • । — 651 0- । • •1 • 1 '• • ■ • । ■ ■ •11 •r ■ • i ■ ■ 1/ miz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #26922: Mercaptoacetic acid, bis(trimethylsily!)- 73 147 34.00 34.20 34.40 34.60 5000 m/z 281.10 34.77% 221

0- 1111 13.334104 f trm Pi 177 I , miz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... Ma MMaha A4 hal yMAMiM” 147 221 34.00 34.20 34.40 34.60 m/z 355.00 27.66% 73 5000

0 TT 28, 117 — 191 29................. ----- n/z—> 0 50 100 150 200 '256' 300 350 400 ' 450 500 55o' 600 650 34.00 34.20 34.40 34.60

11903.D 052202.M Tue May 28 12:07:57 2002 Page 19

NYC-WTC_000012931

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