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GCMS calibration data, Sample 1647, Mar 2002

Machine-extracted title · confidence 100%

Calibration table for GC/MS analysis using Method 625/TCLP recorded on March 12 and 19, 2002.

NYC-WTC_000012200–000012206

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS

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Scanned page image, NYC-WTC_000012203
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

' Data File : C:\HPCHEM\1\DATA\MAR1102\1647.D Vial: 23 Acq On : 12 Mar 2002 12:53 pm Operator: Sample : re-ext fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.303 785 791 802 rBV 806311 1992804 67.38% 12.252% 2 15.939 1181 1187 1203 rBV 1324778 2672811 90.37% 16.432% 3 21.245 1759 1765 1774 rBV 1418507 2872199 97.11% 17.658% 4 25.697 2243 2250 2260 rBV2 1381191 2957625 100.00% 18.183% 5 25.826 2260 2264 2272 rVB 10708 31297 1.06% 0.192%

6 30.765 2797 2802 2809 rBV 209470 406777 13.75% 2.501% 7 33.758 3121 3128 3142 rBV2 1197818 2802985 94.77% 17.233% 8 33.969 3147 3151 3161 rVB 22099 53992 1.83% 0.332% 9 38.026 3583 3593 3609 rBV2 797699 2474974 83.68% 15.216%

Sum of corrected areas: 16265464

1647.D GCMS0308.M Tue Mar 19 09:15:22 2002

NYC-WTC_000012203

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NYC-WTC_000012203Source: NYC Law Department, mirrored locally

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