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GCMS analysis results, Sample AE01640, Mar 2002

Machine-extracted title · confidence 100%

Chromatogram and data from GC/MS analysis of sample AE01640 conducted on March 25, 2002.

NYC-WTC_000012145–000012149

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\MAR1102\1640.D Vial: 21 Acq On : 12 Mar 2002 8:56 am Operator: Sample : re-ext Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 12.304 785 791 806 rVB 745776 1883450 67.56% 12.424% 2 15.940 1181 1187 1201 rBV 1228914 2484137 89.11% 16.386% 3 21.246 1759 1765 1777 rBV 1366707 2720641 97.60% 17.946% 4 25.689 2243 2249 2261 rBV2 1252201 2787647 100.00% 18.388% 5 30.766 2797 2802 2808 rBV 209289 415222 14.90% 2.739%

6 33.759 3121 3128 3147 rBV2 1143743 2614962 93.81% 17.249% 7 38.027 3584 3593 3614 rBV2 725127 2254316 80.87% 14.870%

Sum of corrected areas: 15160375

1640.D GCMS0308.M Tue Mar 19 09:14:25 2002

NYC-WTC_000012147

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NYC-WTC_000012147Source: NYC Law Department, mirrored locally

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