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GCMS Analysis Report, Sample AE04332, Apr 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis report for sample AE04332 conducted on April 1, 2002, including surrogate recovery data.

NYC-WTC_000012008–000012015

Folder label: “GCMS X 2/28/02 A 3/26/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\032602\4332.D Vial: 13 Acq On : 26 Mar 2002 9:00 pm Operator: McLean Sample : 2/28/02 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 9.548 1094 1101 1130 rBV 1955338 5486627 66.17% 12.910% 2 13.021 1685 1692 1713 rBV 3588507 7700956 92.88% 18.120% 3 18.138 2553 2563 2580 rBV 3938074 8273459 99.78% 19.467% 4 22.492 3295 3304 3326 rBV2 3545257 8291408 100.00% 19.510% 5 27.428 4137 4144 4163 rBV 596474 1162460 14.02% 2.735%

6 30.307 4624 4634 4656 rBV2 3157201 7389965 89.13% 17.389% 7 34.179 5283 5293 5316 rBV2 1667044 4194091 50.58% 9.869%

Sum of corrected areas: 42498966

1332.D 5080302.M Wed Mar 27 08:52:11 2002 Page 1

NYC-WTC_000012013

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NYC-WTC_000012013Source: NYC Law Department, mirrored locally

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