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GCMS Analysis Report, Sample AE04335, Apr 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis report for sample AE04335 conducted on April 1, 2002, including surrogate recovery data.

NYC-WTC_000012016–000012023

Folder label: “GCMS X 2/28/02 A 3/26/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

’Data File : C:\MSDCHEM\1\DATA\032602\4335.D Vial: 9 Acq On : 26 Mar 2002 5:43 pm Operator: McLean Sample : 2/28/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal. : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 9.548 1094 1101 1133 rBV 2071864 5590520 69.62% 14.552% 2 13.027 1685 1693 1715 rBV 3739176 7760050 96.64% 20.199% 3 18.138 2554 2563 2583 rBV 3829712 8029996 100.00% 20.902% 4 22.492 3295 3304 3316 rBV2 3217078 7090131 88.30% 18.455% 5 27.428 4137 4144 4158 rBV 441177 920768 11.47% 2.397% 6 30.301 4624 4633 4650 rBV2 2424842 5708294 71.09% 14.859% 7 34.179 5282 5293 5316 rBV 1285959 3317784 41.32% 8.636%

Sum of corrected areas: 38417543

4335.D 5080302.M Wed Mar 27 08:18:35 2002 Page 1

NYC-WTC_000012021

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NYC-WTC_000012021Source: NYC Law Department, mirrored locally

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