NYC-WTC_000011942
Technical record of GCMS calibration data for TCLP analysis using sample vial 13 from March 28, 2002.
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GCMS calibration table for TCLP analysis, March 2002
Machine-extracted title · confidence 100%Technical record of GCMS calibration data for TCLP analysis using sample vial 14 from March 28, 2002.
NYC-WTC_000011949–000011955Folder label: “GCMS X 2/28/02 A 3/26/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) ,P Data File : C:\HPCHEM\l\DATA\MAR2502\4387.D Vial: 14 Acq On : 25 Mar 2002 11:01 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 12:08 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 459724 20.00 ug/1 -0.10 10) Naphthalene-d8 15.88 136 1758627 20.00 ug/1 -0.11 17) Acenaphthene-diO 21.19 164 958255 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.63 188 1382454 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 240 746555 20.00 ug/1 -0.15 44) Perylene-dl2 37.93 264 445280 20.00 ug/1 -0.19
System Monitoring Compounds 5.2" 37) 2,4-DDD 30.71 235 96799 . 554 ug/mL 0.21 Spiked Amount 5.000 Recovery = 171.00%/03
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.94 128 318 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.68 149 450 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 4387.D GCMS0308.M Thu Mar 28 12:10:45 2002 Page 1
NYC-WTC_000011949
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