GCMS analysis results for sample AE04126, April 2002

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Laboratory report documenting GCMS analysis of sample AE04126 conducted on April 1, 2002, by analyst DLV.

NYC-WTC_000011747–000011756

Folder label: “GCMS X 2/25/02 A 3/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4126.D Vial: 22 Acq On : 23 Mar 2002 4:45 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.21 ug/1 36317 Phenanthrene- dl 0 25.65

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 Phenanthre: diO 188 C14D10 001517-22-2 50 2 Naphthal en 1,7-dimethoxy- 188 C12H1202 005309-18-2 42 3 Antipyrine 188 C11H12N2O 000060-80-0 40 4 4-Fluoro-6 mejbhyl-2-phenylpyrimidin 188 C11H9FN2 000000-00-0 40 Abundance 7 Scan 2261 (25.800 min): 4126b (-) ~...............i m/z 188.10 100.00% 1118

5000

42 66 80 94 160 . 25.40 25.60 25.80 26.00 26.20 m/z 189.05 15.06% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-di0 188

) 1 5000 i ■ *-I i • ■ ' ■ i ' • 25.40 25.60 25.80 26.00 26.20 RR 80 94 160 m/z 184.10 10.75% ill j t t । i j i i i I | I I : । । > । । i [ । i । t । I I J t | i I I I [ I I । । [ । i I i । i i । । j i r i i । A

m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 14.12 ... 1 ′ . . • R.5 173 188 11*11*1a iT-1 IIIIIIi 25.40 25.60 25.80 26.00 26.20 5000 m/z 80.05 9.51% 102 115 145 51 63 75 94 130 158 1‘I‘0IOIBuun—unuputpuut_puuueg m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19872: Antipyrine.... .......... ................................. 188 25.40 25.60 25.80 26.00 26.20 96 m/z 159.95 8.21% 5000 77 56 105 ■ ... . .

11"111" 1' 111" I Il 159 173 ■ i'• i ■ ■ “ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ “ ■ ITM i'| 11111 ' 11111 i i " I *' • ’ I *' miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

4126.D GCMS0308.M Wed Mar 27 10:02:26 2002 Page 2

NYC-WTC_000011755

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