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GCMS reference analysis results for sample AE03265, March 2002

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Laboratory report documenting GCMS reference analysis of sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011396–000011406

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

. ©ata File : C:\MSDCHEM\1\DATA\031902\3265FB.D Vial: 34 Acq On : 21 Mar 2002 8:13 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.561 271 274 298 rBV 397033 1242849 5.55% 1.058% 2 9.552 708 714 740 rBV 6265013 15781831 70.50% 13.438% 3 12.056 985 990 1000 rBV 163266 284979 1.27% 0.243% 4 13.035 1091 1098 1111 rBV 10095783 20822958 93.02% 17.731% 5 15.112 1322 1327 1337 rBV2 325380 591372 2.64% 0.504%

6 17.851 1624 1629 1638 rBV 253312 460288 2.06% 0.392% 7 18.151 1654 1662 1666 rBV 9757641 21795653 97.37% 18.559% 8 20.291 1893 1898 1908 rBB 167486 331665 1.48% 0.282% 9 22.396 2124 2130 2135 rBV2 125782 240720 1.08% 0.205% 10 22.514 2135 2143 2147 rBV2 9190023 22384940 100.00% 19.061%

11 22.659 2155 2159 2168 rVB 88491 235248 1.05% 0.200% 12 27.430 2681 2685 2692 rBV 661161 1406286 6.28% 1.197% 13 30.332 2996 3005 3027 rBV2 7283458 20187630 90.18% 17.190% 14 34.196 3423 3431 3447 rBV2 4123787 11674770 52.15% 9.941%

Sum of corrected areas: 117441189

3265FB.D 5080302.M Mon Mar 25 09:02:33 2002 Page 1

NYC-WTC_000011401

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NYC-WTC_000011401Source: NYC Law Department, mirrored locally

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