NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
. 'Data File C:\MSDCHEM\l\DATA\022802\03253.D Vial: 20
Acq On 2 Mar 2002 4:42 am Operator: McLean
Sample 2/13/02 GC SCAN Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: BENZO.P
Quant Time: Apr 02 12:01:17 2002 Quant Results File: 5080202.RES
Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Last Update : Mon Feb 25 19:17:14 2002
Response via : Initial Calibration
DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.58 150 1520929 20.00 ug/L 0.00
10) Naphthalene-d8 13.05 136 3968396 20.00 ug/L 0.00
17) Acenaphthene-dlO 18.17 164 2228141 20.00 ug/L 0.00
29) Phenanthrene-diO 22.52 188 3377595 20.00 ug/L 0.00
38) Chrysene-dl2 30.33 240 3078584 20.00 ug/L -0.03
44) Perylene-dl2 34.21 264 1955530 20.00 ug/L -0.02
System Monitoring Compounds
37) 2,4-ddd surr 27.46 235 218640 4.08 ug/L 0.00
Spiked Amount 5.000 Recovery = 81.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d
3) bis(2-chloroethyl) ether 0.00 93 0 N.D.
4) 1,3 - Dichlorobenze 0.00 146 0 N.D.
5) 1,4 - Dichlorobenzene 0.00 146 0 N.D.
6) 1,2 - Dichlorobenzene 0.00 146 0 N.D.
7) 2,2 1 - oxybis (l-Chloropr 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 0.00 128 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 18.16 165 285323 9.20 ug/L # 25
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 0.00 149 0 N.D.
26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
30) N-Nitrosodiphenylamine 0.00 169 0 N.D.
31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D.
3 2) Hexachlorobenzene 0.00 284 0 N.D.
33) Phenanthrene 0.00 178 0 N.D.
34) Anthracene 0.00 178 0 N.D.
35) Di-n-butylphthalate 24.67 149 84206 0.37 ug/L 98
36) Fluoranthene 0.00 202 0 N.D.
39) Pyrene 0.00 202 0 N.D.
40) Butylbenzylphthalate 0.00 149 0 N.D.
41) Benzo (a) antracene 30.34 228 7932 0.04 ug/L 46 X
42) Bis (2-ethylhexyl) phthala 30.93 149 6447 0.05 ug/L 88 (
43) Chrysene
45) Di-n-Octylphthalate
46) Benzo (b) fluoranthene
30.34
0.00
0.00
228
149
252
7932
0
0
0.04 ug/L
N.D.
N.D.
44 X
(#) = qualifier out of range (m) = manual integration
03253.D 5080202.M Tue Apr 02 12:01:54 2002 Page 1
NYC-WTC_000011221
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