Analytical report showing surrogate recovery data for sample AE03071 analyzed on March 12, 2002.
NYC-WTC_000005947–000005954Folder label: “GCMS X 2/12/02 A 2/28/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File C:\MSDCHEM\l\DATA\022802\03021.D Vial: 14 Acq On 1 Mar 2002 11:00 pm Operator: McLean Sample 2/12/02 GC SCAN Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 04 05:43:58 2002 Quant Results File: 5080202.RES
Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.58 150 1619943 20.00 ug/L 0.00 10) Naphthalene-d8 13.05 136 4285993 20.00 ug/L 0.00 17) Acenaphthene-diO 18.17 164 2383782 20.00 ug/L 0.00 29) Phenanthrene-diO 22.52 188 3657758 20.00 ug/L 0.00 38) Chrysene-dl2 30.34 240 3444966 20.00 ug/L -0.02 44) Perylene-dl2 34.21 264 2287403 20.00 ug/L 0.00
System Monitoring Compounds 37) 2,4-ddd surr 27.46 235 231075 3.98 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 ' - oxybis (1-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2 -chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 24.67 149 3391 0.01 ug/L 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo (a) antracene 30.34 228 9297 0.04 ug/L 56— Y ' 42) Bis (2-ethylhexyl) phthala 43) Chrysene 45) Di-n-Octylphthalate 46) Benzo (b) fluoranthene 30.94 30.34 0.00 0.00 149 228 149 252 12053 9297 0 0 0.08 ug/L 0.04 ug/L N.D. N.D. 96 X 532 • . w (#) = qualifier out of range (m) = manual integration 03021.D 5080202.M Mon Mar 04 05:44:27 2002 Page 1
NYC-WTC_000005949
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NYC-WTC_000005992
Technical comment regarding low recovery rates in GCMS scan of sample AE03016, indicating a decision to reextract and reanalyze the specimen.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005925
Analytical report showing surrogate recovery data for sample AE03020 analyzed on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005963
Analytical report showing surrogate recovery data for sample AE03072 analyzed on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005983
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03074 conducted on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005973
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03073 conducted on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005937
Analytical report showing surrogate recovery data for sample AE03021 analyzed on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006001
Laboratory report documenting GCMS analysis of environmental sample AE03019 conducted on April 3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011298
Laboratory report documenting GCMS analysis of environmental sample AE03259 conducted on April 3, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011319
Laboratory report documenting GCMS analysis of environmental sample AE03263 conducted on April 3, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038721
Laboratory data recording surrogate recovery and unknown compound screening for sample AE04512 dated April 4, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011250
Laboratory report documenting GCMS analysis of environmental sample AE03255 conducted on April 3, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011241
Laboratory report documenting GCMS analysis of environmental sample AE03254 conducted on April 3, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Laboratory report listing recovery percentages for thirteen volatile organic compounds in reference standard AE03017 analyzed on March 4, 2002.
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