GCMS analysis results, sample AE02718, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C: \MSDCHEM\1\5973N\02FEB28\02718.D Vial: 3 Acq On : 28 Feb 2002 4:20 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Butenol, methyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. 5.02 0.07 ug/L 25247 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butenol, methyl- 86 C5H10O 060766-00-9 74 2 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 9 3 Di-iso-amyl oxalate 230 C12H2204 000000-00-0 9 4 3-Buten-2-ol, 2-methyl-86 C5H10O 000115-18-4 7 Abundance Scan 146 (5.022 min): 02718.D (-) m/z 43.10 100.00% 43 71

5000 59 ...... ......

84 4.60 4.80 5.00 5.20 5.40 0- * • । * *»• i *1 > * । > * m/z 71.00 86.81% miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #4093: Butenol, methyl- 43 71

5000 59 i t W. ■ ■ i ■ ■ ■ ■ i ■ ■ 27 4.60 4.80 5.20 5.40 5.00 15 m/z 41.10 58.40% 0- _ tr , 1 ■ i • ■ ■ ‘ r1 1 1 1 " ■ i 86 ■ i ‘ ■ i ■ ■ ■ ' I ' 1 ■ ■ i ■ 1 ■ • i ■ ' ‘ ' i ■ ■ 1 ‘ i ‘ ■

miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #4090:3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 43 71

4.60 4.80 5.00 5.20 5.40 5000 m/z 69.00 , 35.94% 27 59

0- iz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #159394: Di-iso-amyl oxalate ■ ■ i ■ ■ ■ ■ i ' ■ 43 4.60 4.80 5.20 5.40 5.00 71 m/z 59.00 35.46% 5000 55

0 ................. 11 — Ir 87 115 161 188 230 1 • > i • > • • 1 l 1 • ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ I 1 1 ' ■ i ■ ■ ‘ ■ i ■ 1 ■ ■ i ■ ' ■ ■ i ■ /z-> 20 40 60 80 100 120 140 160 180 200 220 4.60 4.80 5.00 5.20 5.40

02718.D HP022102.M Fri Mar 01 10:07:28 2002 Page 9

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