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GCMS sample analysis results for AE01968, March 2002

Machine-extracted title · confidence 100%

Laboratory report detailing the analytical results for sample AE01968 obtained via GCMS on March 22, 2002.

NYC-WTC_000010359–000010373

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\MAR1902\1968.D Vial: 13 Acq On : 20 Mar 2002 4:46 pm Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.267 782 787 805 rVB 1415273 3133650 68.17% 12.099% 2 15.902 1177 1183 1200 rBV 2056224 4233531 92.10% 16.346% 3 21.218 1755 1762 1780 rBV 2193145 4596862 100.00% 17.749% 4 25.661 2239 2246 2257 rBV2 2093210 4476001 97.37% 17.282% 5 30.728 2793 2798 2805 rBV 239019 481358 10.47% 1.859%

6 33.721 3113 3124 3143 rBV2 1426036 3270058 71.14% 12.626% 7 34.970 3253 3260 3269 rBV 52398 151437 3.29% 0.585% 8 36.163 3383 3390 3405 rBV 114191 381588 8.30% 1.473% 9 37.402 3513 3525 3550 rBV 145798 667267 14.52% 2.576% 10 37.972 3579 3587 3610 rBV2 726506 2214186 48.17% 8.549%

11 38.862 3675 3684 3709 rBV2 139582 783392 17.04% 3.025% 12 40.634 3865 3877 3905 rBV2 102366 731405 15.91% 2.824% 13 42.846 4103 4118 4141 rBV2 61125 511173 11.12% 1.974% 14 45.619 4406 4420 4437 rBV4 30580 267572 5.82% 1.033%

Sum of corrected areas: 25899480

1968.D GCMS0308.M Thu Mar 21 09:19:01 2002

NYC-WTC_000010364

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NYC-WTC_000010364Source: NYC Law Department, mirrored locally

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