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GCMS analysis results for sample AE01692, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01692 conducted on March 4, 2002, including surrogate recovery data.

NYC-WTC_000010242–000010248

Folder label: “GCMS X 1/25/02 A 2/25/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\FEB2502\1692.D Vial: 13 Acq On : 25 Feb 2002 11:20 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 12.313 787 792 808 rBV 516736 1285132 72.16% 15.351% 2 15.958 1183 1189 1206 rBV 787454 1683282 94.51% 20.108% 3 21.264 1761 1767 1780 rBV 827707 1781002 100.00% 21.275% 4 25.716 2245 2252 2262 rBV2 696964 1585965 89.05% 18.945% 5 30.793 2800 2805 2811 rVB 82356 155781 8.75% 1.861%

6 33.777 3123 3130 3149 rBV2 462374 1060232 59.53% 12.665% 7 38.046 3585 3595 3615 rBV2 263461 820001 46.04% 9.795%

Sum of corrected areas: 8371395 1692 .D GCMS0208.M Thu Feb 28 09:34:19 2002

NYC-WTC_000010247

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NYC-WTC_000010247Source: NYC Law Department, mirrored locally

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