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GCMS analysis results for sample AE01689, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01689 conducted on March 4, 2002, including surrogate recovery data.

NYC-WTC_000010214–000010221

Folder label: “GCMS X 1/25/02 A 2/25/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB25O2\1689.D Vial: 10 Acq On : 25 Feb 2002 8:23 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.311 787 792 806 rVB 492291 1327123 72.76% 15.631% 2 15.955 1183 1189 1207 rBV 817055 1729946 94.85% 20.376% 3 21.271 1761 1768 1784 rBV 839534 1823930 100.00% 21.483% 4 25.714 2245 2252 2263 rBV2 763201 1609972 88.27% 18.963% 5 30.791 2800 2805 2811 rVB 84950 155920 8.55% 1.836%

6 33.774 3122 3130 3144 rBV2 461025 1048607 57.49% 12.351% 7 38.043 3588 3595 3609 rBV2 261409 794579 43.56% 9.359%

Sum of corrected areas: 8490077

1689.D GCMS0208.M Thu Feb 28 09:32:24 2002

NYC-WTC_000010219

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NYC-WTC_000010219Source: NYC Law Department, mirrored locally

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