GCMS analysis report for sample AE01547, March 2002

NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01547.D Vial: 3 Acq On : 21 Feb 2002 4:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.487* 7 10 15 rBV 23142 41262 0.30% 0.060% 2 3.622 17 22 27 rBV 31956 53615 0.40% 0.078% 3 3.927 47 49 53 rVB 15952 26211 0.19% 0.038% 4 4.379/ 85 89 95 rVB3 8644 19011 0.14% 0.028% 5 5.507/ 185 189 199 rVB3 4066 15127 0.11% 0.022% 6 5.9481/ 227 228 241 rBV2 34007 131922 0.97% 0.192% 7 9.718 557 562 567 rBV 4160196 7975557 58.93% 11.594% 8 13.195 . 865 870 875 rBV 6172248 11714323 86.56% 17.029% 9 883 886 899 _ _____________ rVB2 13670 41156 0.30% 0.060% 10 16.548/ 1163 1167 1171 rW3 11449 18534 0.14% 0.027% 11 18.332 1321 1325 1331 rBV 6086535 12760606 94.29% 18.550% 12 18.738/ 1357 1361 1367 rVB3 3964 13604 0.10% 0.020% 13 19.980% 1465 1471 1477 rBV3 8496 23234 0.17% 0.034% 14 22.283 1671 1675 1681 rBV2 34060 68340 0.50% 0.099% 15 22.633 1701 1706 1711 rBV2 5987251 13533340 100.00% 19.674% 16 24.857/ 1899 1903 1909 rVB 6753 20715 0.15% 0.030% 17 27.724 2153 2157 2163 rBV 799254 1453370 10.74% 2.113% 18 30.490/2397 2402 2449 rBV 5015798 11959849 88.37% 17.386% 19 31.099 2453 2456 2461 rVB 15333 25436 0.19% 0.037% 20 34.407 2743 2749 2787 rBV 3183085 8893404 65.71% 12.929%

Sum of corrected areas: 68788616

01547.D HP022102.M Mon Feb 25 10:55:23 2002 Page 1

NYC-WTC_000010070