GCMS analysis results for sample AE01507, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report J Data File : C:\MSDCHEM\l\5973N\02FEB21\01506.D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

3.50 0.12 ug/L 49292 1,4 -Dichiorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 78 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 43 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 40 Abundance Scan 11 (3.498 min): 01506.D (-) m/ z 74.00 100.00% 74 A 82 5000' 47 ................... 3.50 3.60 3.70 3.80 3.90

miz-> 0+ /* 10 20 30 40 50 I... 60 . 70 80 90 I ■ i ' ■ ■ ■ i.. P 100 110 m/z 81.90 63.47% Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 47 82 N,...... ... .. 3.50 3.60 3.70 3.80 3.90 m/z 47.00 31.29% 35 - _______L , 109 Of ‘ Tnd 1 ' i ■ ■ ■ ■ i 1 ‘ ’ ' 1 1 • 'i ' '

niz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82 3.50 3.60 3.70 3.80 3.90 5000 m/z 83.90 30.87% 47 35 12 Of PP . .. Ill,.,, ■ i 1 ■ ■ ■ i ■ i TIiB 108 ■ i ■ ■ ■ ■ i 1 ' ' 1 I ■ ■ ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 3.50 3.60 3.70 3.80 3.90 35 m/z 75.90 29.21%

5000 82

47

01 • ■ i ■ ■ ■ • i ■ ■ • ‘ i ■ ■ 1 —Ht ■ 1 i ■ ‘ ■ i ■ TI8 1 ■ i • • ‘ ‘ i ' ■ ■ ‘ i ■ ‘ +41444/8144241444424***4* miz—> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90

01506.D HP022102.M Mon Feb 25 10:54:43 2002 Page 3

NYC-WTC_000009952