GCMS analysis results for sample AE01439, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1439.D Vial: 11 Acq On : 21 Feb 2002 11:57 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.29 ug/1 19597 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual ----------------- / I Silane, tetramethyl - 88 C4H12Si 000075-76-3 36 2 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 1,3-Dioxolane 74 C3H602 000646-06-0 7 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 Abundance 7 Scan 345 (8.207 min): 1439.D (-) m/ z 73.00 100.00% 73

5000 43 1**’’I*’1*I’+*II* 7.80 8.00 8.20 8.40 8.60 m/z->______10 ■ • i ■ ■ ■ ■ i ■ ■ ■ ' i • 20 30 —40ll 50 51 , 59 i i 1 i‘ *4 ■ i ■ ■ ■ ■ i • 60 70 i 80 87 90 100 110 120 m/ z 43.05 28.97% Abundance #62932: Silane, tetramethyl-

... V.. 73

5000 7.80 8.00 8.20 8.40 8.60 45 m/z 41.05 12.46% 15 53 59 88 ■ . J .... । | i > j [ I ! 1 < j i'i'i'I'i i । ' 1 i ' ■ ■ ■ i ' ' ■ ' i ' ■ 1 • i ■ ■ • ‘ i ■ ■ ■ 1 i ■ ■ m&-> 10 20 30 40 50 60 . 70 80 90 100 110 120 Abundance .‘ 73 I.... I ‘ ‘ ' I ' ‘ ‘ I ‘ ‘ 1 1 1 1 1 1 1 I 1 1 7.80 8.00 8.20 8.40 8.60 5000 m/ z 45.05 12.31% 45 36 67 55 109115 ■ ' i ' ■ ■ ‘ i ■ ■ ■ ■ i ' ■ ■ ■ i ■ 1 1 1 i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ • * i • ■ ■ ' i ■ ■ ' 1 I 1 1 1 1 1 1 1 ' 1 I ' 1 miz-____ 10___ 20____ 30 -40___ 50 60 70___ 80 90 100 110 120 Abundance ’ ...... ‘ ...... “ #62555:1,3-Dioxolane 73 i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • 1 1 i 1 1 ' 1 i 1 1 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.31% 5000 44 29 .............. ,,...... .11 ■ ' i ' ■ ■ • i 11 1' r1"'' ■ । ii' ' I ■ 57 I 1 1 1 ' I ' --------------- m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40 8.60

1439.D GCMS0208.M Fri Feb 22 09:33:25 2002 Page 1

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