GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

• Data File : C:\HPCHEM\l\DATA\FEB2102\472.D Vial: 6 Acq On : 21 Feb 2002 7:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 22 9:08 2002 Quant Results File: GCMS8208.

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 250732 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 954144 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.29 164 501735 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.73 188 675617 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 410058 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 264490 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 30.81 235 35336 4.52 ug/mL 0.31 Spiked Amount 5.000 Recovery = 90.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Ac enapht hylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 472.D GCMS0208.M Fri Feb 22 09:09:18 2002 Page 1

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