GCMS analysis report for sample AE01224, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1502\1224.D Vial: 33 Acq On : 17 Feb 2002 12:24 am Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.29 ug/1 26488 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual /______________ 1 N-Ethylformamide 73 C3H7NO 000627-45-2 4 2 3,4-Dimethyl-5-hexen-3-ol 128 C8H160 000000-00-0 4 3 Propane,/2-methoxy-2-methyl- 88 C5H120 001634-04-4 4 4 Pentane/ 3-methoxy­ 102 C6H140 036839-67-5 4 Abundance ( Scan 345 (8.213 min): 1224.D (-) m/z 73.00 100.00% 73

5000- 43 ........ )...... 7.80 8.00 8.20 8.40 8.60 ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ 35 11/1 49 55,..........1 , 84 11 ‘1 1,1 1 1 1 111 1 1 1 1 1 i‘ I ■ ■ । 1 1 103 • i • • ■ > i <’• • > i ■ m/z 43.05 42.87% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 44 58 7.80 8.00 8.20 8.40 8.60 m/ z 41.05 14.55% 15 i ■ ■ ■ ■ r1 1 1 1 i 1 1 1 1 i 1 1 1 1 i 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 73 ......... .......... । ■ 1 । ■ ' ' ■ । ■ 1 1 i 1 Tun— i 1 1 43 7.80 8.00 8.20 8.40 8.60 5000 55 m/ z 44.95 14.17% 27 67 81 99 ‘ ' i 1 1 1 ‘ i ‘ ' ' i ■ ' ' ■ i ' 1 1 1 1 1 ' 1 1 1 1 1 1 ' i ' ‘ ‘ ' i ' ‘ ' i ' ‘ ' ■ i ‘ 1 ‘ ' i ' m/z-> 10 20 .... 30 40 50 60 70 80 90 100 110 Abundance #62967: Propane, 2-methoxy-2-methyl- 73 7.80 8.00 8.20 8.40 8.60 m/z 39.05 9.14% 5000

41 57

15 ■ 1 i ' ' ‘ ■ i ‘ 2733 1 ,................... ' ■ i ■ ‘ ■ ■ i 1 ' 1 1 1 1 ' 1 1 1 1 1 1 1 1 1 I m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1224.D GCMS0208.M Thu Feb 21 09:29:57 2002 Page 1

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