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← Document results/DEP Box 13/508 Xtract 10/11/01 Analyzed 11/10/11
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GC/MS data: toxaphene analysis, Nov 2001

Machine-extracted title · confidence 95%

Instrument data file showing signal responses and recovery percentages for toxaphene peaks in sample AD24395.

NYC-WTC_000007034–000007035

Folder label: “508 Xtract 10/11/01 Analyzed 11/10/11

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Signal #1 : C:\HPCHEM\1\DATA\508F\011110\24395SDT.D\ECD1A.CH Vial: 96 Signal #2 : C:\HPCHEM\1\DATA\508F\011110\24395SDT.D\ECD2B.CH Acq On : 13 Nov 2001 4:22 pm Operator: Nefliu Sample : 24395 spike dupe tox Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Nov 15 9:20 2001 Quant Results File: 011115T.RES Quant Method : C:\HPCHEM\1\METHODS\011115T.M (Chemstation Integrator) Title : 508 CHLORINATED PESTICIDES TOXAPHENE7/28/99 Last Update : Fri Nov 09 16:13:01 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 6) S 2,4-DDD SURROGAT 0.00 33.74 0 599308 N.D. 0.102 # Spiked Amount 0.200 Recovery = 0.00% 51.00% Target Compounds 1) TOXAPHENE PEAK 1 35.22 0.00 50954 0 1.219 N.D. d# 2) TOXAPHENE PEAK 2 0.00 36.42 0 219367 N.D. 2.052 # 3) TOXAPHENE PEAK 3 0.00 37.99f 0 4568 N.D. 0.059 # 4) TOXAPHENE PEAK 4 45.32 39.83f 154545 27606 0.966 0.246 # 5) TOXAPHENE PEAK 5 0.00 40.47 0 22779 N.D. 0.287 #

J

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 24395SDT.D 011115T.M Thu Nov 15 09:20:53 2001 Page 1

NYC-WTC_000007034

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NYC-WTC_000007034Source: NYC Law Department, mirrored locally

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