NYC-WTC_000006328
Initial GCMS analysis report for sample AE03435 conducted by analyst DLV on March 12, 2002.
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GCMS Sample AE03390 Report, March 12 2002
Machine-extracted title · confidence 95%Initial GCMS analysis report for sample AE03390 conducted by analyst DLV on March 12, 2002.
NYC-WTC_000006311–000006318Folder label: “GCMS X 2/14/02 A 2/23/02”
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DA*r{ owed)
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\FEB2102\3390.D Vial: 52 Acq On : 23 Feb 2002 7:20 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 8 9:27 2002 Quant < Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.33 152 228436 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 884113 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.29 164 466859 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.73 188 667561 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 463159 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 312918 20.00 ug/1 -0.04
System Monitoring Compounds 31 37) 2,4-DDD 30.81 235 46051 6.61 ug/mL 0.31 Spiked Amount 5.000 Recovery = 132.20% 70%
Target Campounds Qvalue 2) N-ntroso-dimethyl amine 0.00 74 0 N.D. 3) bis 6-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-)ichlorobenzene 0.00 146 0 N.D. 5) 1,4-ichlorobenzene 0.00 146 0 N.D. 6) 1,2-ichlorobenzene 0.00 146 0 N.D. 7) 2,2 ‘oxybis (1-Chloropropan 0.00 45 0 N.D. 8) N-Nioso-di-n-propylamine 0.00 70 0 N.D. 9) Hexaloroethane 0.00 117 0 N.D. 11) Nitrnzene 0.00 77 0 N.D. 12) Isopone 0.00 82 0 N.D. 13) bis (Zhloroethoxy) methane 0.00 93 0 N.D. 14) lf2,4richlorobenzene 0.00 180 0 N.D. 15) Naphtlene 0.00 128 0 N.D. 16) Hexacorobutadiene 0.00 225 0 N.D. 18) Hexacrocyclopentadiene 0.00 237 0 N.D. 19) 2-Chlonaphthalene 0.00 162 0 N.D. 20) Dimetphthalate 0.00 163 0 N.D. ’1) 2,6-Ditrotoluene 0.00 165 0 N.D. 12) Acenapylene 0.00 152 0 N.D. :3) Acenapene 0.00 153 0 N.D. 4) 2,4-Dirotoluene 0.00 165 0 N.D. 5) Diethythalate 22.77 149 365 N.D. 6) 4-Chlohenyl -phenylether 0.00 204 0 N.D. 7) Fluorei 0.00 166 0 N.D. 8) Azoben 1,2-Diphenylhyd 0.00 77 0 N.D.
) = <qualif out of range (m) = manual integration 30.D GCMS3 . M Fri Mar 08 09:34:09 2002 Page 1
NYC-WTC_000006313
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