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GCMS blank sample results, Mar 8 2002

Machine-extracted title · confidence 95%

Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank quality control sample.

NYC-WTC_000006261–000006271

Folder label: “GCMS X 2/14/02 A 2/23/02

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Scanned page image, NYC-WTC_000006262
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB2102\LBC.D Vial: 44 Acq On : 23 Feb 2002 11:27 am Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 8 9:04 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 234254 20.00 ug/1 -0.03 10) Naphthalene-d8 15.97 136 895463 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.29 164 483806 20.00 ug/1 -0.03 29) Phenanthrene-diO 25.73 188 670877 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 430203 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 283269 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 30.82 235 47220 3.3° 6--74 ug/mL 0.32 Spiked Amount 5.000 Recovery 134. 80% 787

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.97 74 570 N.D. 3) bis(2-Chloroethyl)ether 11.72 93 823 N.D. 4) 1,3-Dichlorobenzene 12.23 146 560 N.D. 5) 1,4-Dichlorobenzene 12.37 146 776 N.D. 6) 1,2-Dichlorobenzene 12.90 146 758 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 14.03 77 536 N.D. 12) Isophorone 14.68 82 1277 N.D. 13) bis(2-Chloroethoxy)methane 15.35 93 577 N.D. 14) 1,2,4-Trichlorobenzene 15.85 180 541 N.D. 15) Naphthalene 16.03 128 2883 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.54 162 1066 N.D. 20) Dimethylphthalate 20.64 163 1443 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 20.82 152 1694 N.D. 23) Acenaphthene 21.37 153 1514 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.77 149 1640 N.D. 26) 4-Chlorophenyl-phenylether 22.93 204 496 N.D. 27) Fluorene 22.90 166 1433 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

#) = qualifier out of range (m) = manual integration BC.D GCMS0208.M Fri Mar 08 09:07:01 2002 Page 1

NYC-WTC_000006262

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NYC-WTC_000006262Source: NYC Law Department, mirrored locally

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