GCMS reference standard results, sample AE03017, March 2002

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Data File : C:\MSDCHEM\1\DATA\0 2 2 8 0 2\CAL4 OX.D Vial: 2 Acq On : 28 Feb 2002 10:56 am Operator: McLean Sample : CAL 40 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 4 5:55 2002 Quant Results File: 5080202.RES Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Feb 25 19:17:14 2002 Response via : Initial Calibration Abundance TIC: CAL40X.D

1.7e+07

1.6e+07 aa

ig 1.5e+07 9 to a o s 1.4e+07 s £ 8 6 a s 1.3e+07 3 8 % © 8 8 1 s Z o 5 g 8 o I5 E © o £ § s. S & 0) ra © e © t g I N 8« 8 o fs s§ 5§ 4 5 g 3 iR m 5 5 s 8 m £

t © § 9 s 8 4) 5 © 5 s8 h C 1.2e+07 a' as § 8 § S' 5 § 8 § 2 5 l' 4) £ 3 I 8 Eg 5 § § 2 g 1 h 1.1e+07 85 88 8 CD Q£ 5 IQ o5 8a B 3 Q d 85 88 8 3 ?c 2 £ & a X v 85 8 r s8 4 1e+07

9000000 & 5- 6 2 is 18fl 1!83 I 0) o 8 8

3 f II. 5 I 8 1 X o 3 B 1 8000000 o } C 5 & 4) 5 5 13 2 & © 3 6 5 i o & 88 7000000 G ip 2 ? 8

f I J 8 E J £ 1 m& 1- a s $8 6000000 f 2 x s I I C Q

5000000' t s 11 C CD E 4000000 15 2 i © CD

O o 3000000 Q co O. t 2000000 O o CO Q LO o o 1000000 o o o Q Time-> 0T - —I -* 4.00 6.00 --T 8.00 10.00 12.00 14.00 4 UT 16.00 ¥ 18.00 TI 1 4 20.00 22.00 AUU W A, - La 24.00 26.00 —t —41 28.00 30.00 32.00 —

34.00 1 438.00 36.00 ■ i * o o o I

o CAL40X.D 5080202.M Mon Mar 04 05:56:09 2002 Page 3 Id O > > 7 7