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GCMS analysis results for sample AD30645, Feb 2002

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Gas chromatography-mass spectrometry analysis of environmental sample AD30645 conducted on February 15, 2002.

NYC-WTC_000005804–000005811

Folder label: “GCMS X 2/11/02 A 2/13/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB1302\30645.D Vial: 10 Acq On : 13 Feb 2002 11:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 10:04 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.75 178 234 N.D. 34) Anthracene 25.75 178 234 N.D. 35) Di-n-butylphthalate 27.71 149 12350 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.82 228 1763 N.D. 42) Bis(2-ethylhexyl)phthalate 34.02 149 720 N.D. 43) Chrysene 33.90 228 547 N.D. 45) Di-n-Octylphthalate 35.75 149 291 N.D. 4 6) Benzo(b)fluoranthene 36.89 252 701 N.D. 47) Benzo(k)fluoranthene 36.95 252 743 N.D. 4 8) Benzo(a)pyrene 38.10 252 1480 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30645.D GCMS0208.M Fri Feb 15 10:05:10 2002 Page 2

NYC-WTC_000005807

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NYC-WTC_000005807Source: NYC Law Department, mirrored locally

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