GCMS analysis results for sample AE02645, Mar 15, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR0702\2645.D Vial: 18 Acq On : 8 Mar 2002 6:27 am Operator: Sample : gc/ms scan 2/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 11 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

32.35 0.30 ug/1 55446 Chrysene-dl2 33.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 47 2 l,l,l,5,7,7,7-Heptzhmethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 37 3 3-Isopropoxy-1,1/1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 4 1-Monolinoleoy lycerol. trimethylsi . . .■ 498 C27H5404Si2 m/z 054284-45-6 25 Abundance Scan 2974 (32.347 min): 2645.D (-) 73.00 100.00% 73

5000 147 221 231 । Jbb 32.00 32.20 32.40 32.60 45 ' 'I * ' , 191| . , ,327, I , 429 m/z 147.00 43.14% m/z-2 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,115,5,5-hexamelhyl-3,3-bisi(trimet 73 147 281 5000 32.00 32.20 32.40 32.60 369 m/z 221.05 28.68% 207 249 338 1.................. ■ ' i ■ ' ' ■ i ' ■ m/Z— 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 ................................ .........................

147 32.00 32.20 32.40 32.60 5000 267 m/z 281.10 21.77% 355 429 45 207

m/z->... 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-sopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ■ ■ i ■ 1 1 1 i ■ ■ • 1 i 1 ■ 1 1 i ■ 73 32.00 32.20 32.40 32.60 m/z 355.05 15.78% 5000 147

221 281 307 A4c , ,347 ........ 415............ 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 32.00 32.20 32.40 32.60

2645.D GCMS0208.M Wed Mar 13 14:54:48 2002 Page 11

NYC-WTC_000005432