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GCMS blank analysis results, Mar 13, 2002

Machine-extracted title · confidence 90%

Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.

NYC-WTC_000005367–000005382

Folder label: “GCMS X 2/5/02 A 3/7/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0 70 2\LB.D Vial: 15 Acq On 8 Mar 2002 3:29 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 14:21 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.69 178 364 N.D. 34) Anthracene 25.69 178 364 N.D. 35) Di-n-butylphthalate 27.66 149 20245 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.35 149 187 N.D. 41) Benzo(a)anthracene 33.76 228 2492 N.D. 42) Bis(2-ethylhexyl)phthalate 33.97 149 2909 N.D. 43) Chrysene 33.76 228 2491 N.D. 45) Di-n-Octylphthalate 36.17 149 1038 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 38.02 252 3172 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0208.M Wed Mar 13 14:23:26 2002 Page 2

NYC-WTC_000005369

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NYC-WTC_000005369Source: NYC Law Department, mirrored locally

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