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GCMS analysis results for sample AE02603, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02603 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005333–000005343

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005338
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document UDU Mica L C L CCIIL REpOL L

Data File C:\HPCHEM\1\DATA\MAR0102\2603.D Vial: 13 Acq On 1 Mar 2002 8:10 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.246 127 131 142 rVB2 11314 23725 1.01% 0.197% 2 8.201 339 344 353 rBV 11875 30768 1.31% 0.256% 3 12.314 787 792 808 rVB 684167 1602155 68.37% 13.322% 4 15.959 1182 1189 1203 rBV 944058 2152029 91.84% 17.894% 5 21.265 1761 1767 1781 rBV 1021480 2343212 100.00% 19.484%

6 25.717 2245 2252 2264 rBV2 1006871 2270272 96.89% 18.877% 7 25.855 2264 2267 2276 rVB 9756 27538 1.18% 0.229% 8 30.794 2800 2805 2814 rVB 149639 303932 12.97% 2.527% 9 33.787 3124 3131 3146 rBV2 741440 1809453 77.22% 15.045% 10 38.056 3587 3596 3620 rBV2 451469 1463465 62.46% 12.169%

Sum of corrected areas: 12026549

2603.D GCMS0208.M Mon Mar 04 11:47:15 2002

NYC-WTC_000005338

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NYC-WTC_000005338Source: NYC Law Department, mirrored locally

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