NYC-WTC_000005184
Analytical report listing detected unknown compounds and surrogate recovery results from GCMS testing.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GCMS analysis results for sample AD31132, Feb 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AD31132 conducted on February 11, 2002, including surrogate recovery data.
NYC-WTC_000005229–000005238Folder label: “GCMS X 2/4/02 A 2/8/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\FEBO 802\31132.D Vial: 14 Acq On 8 Feb 2002 9:59 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GQOFY.P Quant Time: Feb 11 12:22 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 12.35 152 278837 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1058778 20.00 ug/1 0.00 17) Acenaphthene-diO 21.31 164 572436 20.00 ug/1 0.00 29) Phenanthrene-diO 25.75 188 819395 20.00 ug/1 -0.02 38) Chrysene-dl2 33.82 240 545130 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 352032 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.84 235 40067 3.93 ug/mL 0.34 Spiked Amount 5.000 Recovery = 78.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.04 128 243 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 31132.D GCMS0208.M Mon Feb 11 12:23:09 2002 Page 1
NYC-WTC_000005231
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