GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\00028A.D Vial: 4 Acq On 5 Feb 2002 5:27 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP020702.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.488 7 10 15 rVB 37804 58189 0.23% 0.045% 2 3.602 17 20 25 rBV 47021 73723 0.30% 0.057% 3 4.230 71 75 79 rBV 241678 383371 1.54% 0.294% 4 5.920 221 223 229 rBV 72689 157009 0.63% 0.120% 5 9.539 535 540 545 rBV 45413 106955 0.43% 0.082%

6 9.630 545 548 551 rW 53611 119950 0.48% 0.092% 7 9.710 551 555 561 rW 7206529 14617884 58.87% 11.205% 8 9.836 561 566 579 rW 68226 224684 0.90% 0.172% 9 13.204 855 861 865 rBV 10188910 21060395 84.81% 16.143% 10 13.375 873 876 881 rVB 24383 45992 0.19% 0.035%

11 16.549 1149 1154 1159 rW 33894 59272 0.24% 0.045% 12 18.353 1305 1312 1317 rBV 9982155 23169926 93.31% 17.760% 13 22.280 1651 1656 1661 rW2 115451 216074 0.87% 0.166% 14 22.440 1667 1670 1673 rBV 29232 49358 0.20% 0.038% 15 22.645 1681 1688 1693 rBV2 9862584 24831311 100.00% 19.033%

16 22.771 1697 1699 1729 rVB 160109 530721 2.14% 0.407% 17 27.726 2129 2133 2139 rBV 1281244 2288976 9.22% 1.754% 18 29.690 2301 2305 2311 rW3 11966 41349 0.17% 0.032% 19 30.512 2369 2377 2407 rBV 8157344 23418247 94.31% 17.950% 20 34.428 2713 2720 2761 rBV 6316590 19010789 76.56% 14.572%

Sum of corrected areas: 130464175

00028A.D HP020702.M Thu Feb 21 15:48:52 2002 Page 1

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