GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00004A.D Vial: 3 Acq On 5 Feb 2002 4:36 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Propanol, 1-(2-methoxypro... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 9.84 0.27 ug/L 218512 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 TRIPROPYLENE GLYCOL 2 192 C9H20O4 000000-00-0 78 3 1-Propanol, 2-(2-hydroxypropoxy) ... 134 C6H14O3 000106-62-7 64 4 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 56 Abundance Scan 566 (9.836 min): 00004A.D (-) m/ z 59.05 100.00% 59

m/z-> 5000

O^r 30 45 73 ,.....'ll.. 111/84......... 'I"...................... 40 50 60 70 80 90 100 110 120 130 140 150 160 104 I..... yJ _ 9.40 9,60 9.80 10.00 10,20 m/Z 45.10 11.41%

Abundance #43942: 2-Propanol, 1-(2-methoxypropoxy)-$$ 1-(2-Methoxyp... 59

5000 UK 1 * 1 1 1 1 1 9.40 m/z 9.60 9.80 73.10 1 ' I ' ' 10.00 10.20 8.53% 31 45 0- —h +ri/ll,..... l U. 73........... 104.........130 1 i1 ■ ■ ■ i' * •' i ■ 1 ■ 1 i1 11 1 r 1 11 i1 1 ■ 1 i' i ‘ ' i ' • • 1 i ' ' ' ' i

MUA... m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #102327: TRIPROPYLENE GLYCOL 2 59 9.40 9,60 9.80 10,00 10.20 5000 m/z 104.10 8.25%

45 103

0- ............ 1111111172 .....89.... Is ■ । * 117 1 130 161 । 1 1 ‘ 1 I 1 1 1 1 i 1 1 1 1 i 1 1 1 1 i ' 1 1 1 i miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #29195:1-Propanol, 2-(2-hydroxypropoxy)- $$ 2-(2-Hydroxyp... 59 9.40 9,60 9,80 10,00 10.20 m/z 42.10 7.88%

5000 31 45 103

n/z-> 0 1 1 I' 30 40 50 75 89 —— 111 ri 1 p ■ ■ ' i ■ ■ ■ ■ । ■1' ■ ।' ‘। ■11 ■ ■'' । ■1 ■ ■ । ■1' ■ । ■ ■ ■' । 60 70 80 90 100 110 120 130 140 150 160 A 9,40 9.60 9,80 10,00 10.20

00004A.D HP020702.M Thu Feb 21 15:48:47 2002 Page 9

NYC-WTC_000004832

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