GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB05\00004A.D Vial: 3 Acq On 5 Feb 2002 4:36 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ******************************************************************* * * Peak Number 6 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

9.63 0.15 ug/L 121459 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H16O3 020324-32-7 72 2 DIPROPYLENEGLYCOL METHYL ETHER $... 148 C7H16O3 020324-32-7 72 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 50 4 BIS(1-METHYL-2-HYDROXYETHYL)ETHER 134 C6H1403 000000-00-0 50 Abundance Scan 548 (9.630 min): 00004A.D (-) m/z 59.05 100.00% 59

Tl/Z-> 5000

0- ■ ■ j ■ ।1111 • ■ ■ । ■ 39 10 20 30 1111 40 45

... Il . 73

50 60 70 80 90 100 110 120 130 140 103

i ■ ■ ■ ■ i ■ 1 Ml I | । । 1 J | 1 * 9.20 9.40 9.60 9.80 10.00 m/ Z 45.10 50.19% Abundance #43943:2-Propanol, 1-(2-methoxy-1-methylethoxy)-$$ Dipro... 59

5000

31 45 73 103 9.20 9.40 m/z 103.05i 9.60 A 9.80 45.97% 10.00

0------ 130 । ■ ■ ■ ■ । ■ ■ ■ ■ । • Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #43944: DIPROPYLENEGLYCOL METHYL ETHER $$ 2-Propanol, 1 -(2... 59 103 9.20 9.40 9.60 9.80 10.00 M. 5000 m/z 73.05 29.43% 45 73 31

0 ■ ■ । 15। । ■ ■ • ■ । ■ —H 1. 11 130 - I ■ t ■ | ■ i n-| ■ ■ ■ . I ■ . ■ ■ । i

. N, A. ■ ■ । ■ ■ • ■ । । mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #61826:2-Butanol, 3,3‘-oxybis- 59 9.20 9.40 9.60 9.80 10.00 m/ z 41.10 23.11%

5000 31 45 103

n/z-> -4 I+ 0 ■' 1 I ' 1 1 'Tri 11 1' 1 10 20 30 40 50 T' ■ ■ ■ i 1 ■ ■ ■ i■ ■ ‘

60 70 80 । ■ 1 ' ' i '

90 100 134 111111 ■' i11111111111 110 120 130 140 .A....... 9.20 9.40 9.60 9.80 10.00

00004A.D HP020702.M Thu Feb 21 15:48:47 2002 Page 8

NYC-WTC_000004831

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