GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\MSDCHEM\1\5973N\02FEB05\00004A.D Vial: 3 Acq On 5 Feb 2002 4:36 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP020702.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.613 19 21 27 rBV 40981 75040 0.29% 0.053% 2 3.933 45 49 53 rVB 23813 42323 0.16% 0.030% 3 4.241 71 76 81 rBV 269819 437371 1.67% 0.311% 4 5.920 221 223 229 rBV 74567 170099 0.65% 0.121% 5 9.539 537 540 545 rBV 49374 112783 0.43% 0.080%

6 9.630 545 548 551 rW 52534 121459 0.46% 0.086% 7 9.710 551 555 561 rW 8059845 15932881 60.78% 11.331% 8 9.836 561 566 579 rW 69065 218512 0.83% 0.155% 9 13.204 855 861 865 rBV 10518449 22481137 85.76% 15.987% 10 13.375 873 876 891 rVB 29680 72215 0.28% 0.051%

11 16.549 1149 1154 1157 rW 33234 60995 0.23% 0.043% 12 18.341 1305 1311 1317 rBV 10188717 24323386 92.78% 17.298% 13 18.421 1317 1318 1337 rVB5 29261 131819 0.50% 0.094% 14 22.280 1651 1656 1661 rBV2 124114 231903 0.88% 0.165% 15 22.645 1681 1688 1693 rBV2 9937381 26214973 100.00% 18.643%

16 22.771 1697 1699 1719 rVB 175447 517863 1.98% 0.368% 17 27.726 2129 2133 2139 rBV 1265871 2275212 8.68% 1.618% 18 29.690 2301 2305 2315 rBV 15144 52379 0.20% 0.037% 19 30.512 2369 2377 2409 rBV2 8841306 25480454 97.20% 18.120% 20 34.428 2713 2720 2767 rBV2 6771611 21664631 82.64% 15.407%

Sum of corrected areas: 140617435

00004A.D HP020702.M Thu Feb 21 15:48:46 2002 Page 1

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