GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02FEB05\30644A.D Vial: 1 Acq On 5 Feb 2002 2:56 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.488 7 10 13 rBV 36625 51779 0.20% 0.039% 2 3.613 19 21 25 rW 37471 62497 0.25% 0.048% 3 4.230 71 75 85 rW 195433 344873 1.36% 0.263% 4 5.920 219 223 229 rBV 72192 157518 0.62% 0.120% 5 5.999 229 230 235 rW 33453 56743 0.22% 0.043%

6 9.550 539 541 547 rW 22434 58705 0.23% 0.045% 7 9.641 547 549 551 rW2 24676 53269 0.21% 0.041% 8 9.710 551 555 561 rW 7212750 14405849 56.86% 10.984% 9 9.847 561 567 579 rW 31021 138047 0.54% 0.105% 10 13.204 855 861 865 rBV 9587742 20535490 81.05% 15.658%

11 13.375 873 876 885 rVB2 24439 54249 0.21% 0.041% 12 16.549 1151 1154 1159 rVB 28816 48658 0.19% 0.037% 13 18.341 1305 1311 1317 rBV 9996001 22931743 90.51% 17.485% 14 22.280 1651 1656 1661 rBV 123074 227937 0.90% 0.174% 15 22.645 1681 1688 1693 rBV2 9850125 25335472 100.00% 19.317%

16 22.771 1697 1699 1709 rVB 157399 372732 1.47% 0.284% 17 27.726 2127 2133 2139 rBV 1255850 2254852 8.90% 1.719% 18 29.690 2299 2305 2317 rW2 14962 55231 0.22% 0.042% 19 30.512 2369 2377 2419 rBV 8481793 24362455 96.16% 18.575% 20 34.428 2713 2720 2761 rBV 6600036 19646152 77.54% 14.979%

Sum of corrected areas: 131154251

30644A.D SCAN508.M Fri Feb 22 11:44:23 2002 Page 1

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