DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB26\02084.D Vial: 1 Acq On : 26 Feb 2002 2:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 4 3-Buten-2-ol, 2,3-dimethyl-... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 4.38 0.05 ug/L 21564 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2,3-dimethyl- (CAS... 100 C6H12O 010473-13-9 17 2 Methacrylamide $$ 2-Propenamide,... 85 C4H7NO 000079-39-0 9 3 1,6-Heptadien-3-yne 92 C7H8 005150-80-1 7 4 1,6-Heptadien-3-yne 92 C7H8 005150-80-1 7 Abundance Scan 89 (4.379 min): 02084.D (-) m/z 91.00 100.00% 91

43 85 5000

51 4.00 4.20 4.40 4.60 4.80

m/z-> mm 11 Of 1’1’22111111000111111111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 1' i1" 11 ■1" i'1 m/z 43.10 62.95% Abundance #8442: 3-Buten-2-ol, 2,3-dimethyl- (CAS) $$ 1-BUTEN-3-OL,... 59 85 43

5000 1 i ■ * 1 1 । 1 ' 1 i 1 1 1 i 1 1 1 i 1 4.00 4.20 4.40 4.60 4.80 m/z 85.00 54.80% 0 "i""i""i•"'i" i" " r ■" i' i'" 11" " I' ’" i " '' i " —, mmmT 100 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3602: Methacrylamide $$ 2-Propenamide, 2-methyl- $$ .alph... 41 85 .............. A.., 4.00 4.20 4.40 4.60 4.80 5000 m/z 92.00 50.10% 69

46 53 0! "i""i" m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #5557:1,6-Heptadien-3-yne 91 4.00 4.20 4.40 4.60 4.80 m/ Z 41.10 32.15% 5000 65 27 51

m/z-> 0 ।1'" ।'। —l..... 37 tm+ip ' 111 H I 1111 11! I.. . i । 1 r " i " 11 r 1" r ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 86 A-4-— WAAAMAA 4.00 4.20 4.40 4.60 4.80

02084.D HP022102.M Wed Feb 27 08:34:46 2002 Page 6

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