Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\JAN2 502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
20.08 3.83 ug/1 3464580 Ac enapht hene-dlO 20.36
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Trisiloxane,1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 12 4 Octadecanic acid, 2- [ (trimethylsil 3 86 C22H4603 S i 056196-58-8 10 Abundance Scan 1638 (20.084 min): 30651.D (-) m/z 7 3 .00 100.00% 73
5000 147 281 327 19.80 20.00 20.20 20.40 45 117 0- TIP 191 221 251 PPPTTTr .. 355,383 415 ....... m/z 147.00 36.17% m/z-> Abundance 50 100 150 200 250 300 350 400 450 500 550 #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim I 73
- 5000 147 19.80 20.00 20.20 20.40 221 m/ z 281.00 33.05% 281l 327 l I 415 519 ■ i561 ■ > i < • ' ■ i ■ > > ■ i < • m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459 Trisifoxane, 1,1,1.5.5.5-hexamethyl-3.3-bisiitnmet 73 147 281 19.80 20.00 20.20 20.40 5000 m/z 326.90 13.37% 207 , 369 .. .... .... 249 ). 338 J, , , ........ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317: 4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 19.80 20.00 20.20 20.40 m/z 282.00 9.74% 327 5000 237 45
miz-> 147172 212 1 'i ■ ‘ 1 ' i ' ' ‘ ■ i ' ' ' ' i 1 50 100 150 200 250 300 l ................. 350 400 450 500 550 4 19.80 20.00 20.20 20.40
30651.D GCMS1126.M Mon Jan 28 12:23:25 2002 Page 6
NYC-WTC_000004226
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
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GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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