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DEP GCMS unknown compounds report, Mar 2002

Machine-extracted title · confidence 95%

GCMS analysis report dated March 6, 2002, listing other unknown compounds and surrogate recovery data for a different sample.

NYC-WTC_000003784–000003793

Folder label: “GCMS X 1/25/02 A 2/26/02

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Scanned page image, NYC-WTC_000003789
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB2502\1799.D Vial: 25 Acq On : 26 Feb 2002 11:34 am Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.201 340 344 353 rBV 10228 24050 1.14% 0.229% 2 12.313 787 792 807 rBV 612027 1482820 70.43% 14.104% 3 15.958 1183 1189 1206 rBV 925605 1966143 93.39% 18.701% 4 21.264 1761 1767 1781 rBV 965073 2105342 100.00% 20.025% 5 25.717 2245 2252 2263 rBV2 910836 1961194 93.15% 18.654%

6 30.793 2800 2805 2812 rBV 114689 225999 10.73% 2.150% 7 33.410 3085 3090 3097 rBV 42281 104187 4.95% 0.991% 8 33.777 3124 3130 3148 rBV2 617177 1484156 70.49% 14.117% 9 38.055 3586 3596 3614 rBV2 375255 1159567 55.08% 11.029%

Sum of corrected areas: 10513458

1799.D GCMS0208.M Thu Feb 28 11:56:52 2002

NYC-WTC_000003789

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NYC-WTC_000003789Source: NYC Law Department, mirrored locally

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