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DEP GCMS unknown compounds report, Mar 2002

Machine-extracted title · confidence 95%

GCMS analysis report dated March 6, 2002, listing other unknown compounds and surrogate recovery data for a different sample.

NYC-WTC_000003744–000003752

Folder label: “GCMS X 1/25/02 A 2/26/02

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Scanned page image, NYC-WTC_000003749
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB2502\1797.D Vial: 23 Acq On : 26 Feb 2002 9:11 am Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.311 787 792 810 rBV 520113 1370158 72.37% 14.765% 2 15.956 1183 1189 1201 rBV 831612 1778767 93.95% 19.168% 3 21.271 1761 1768 1791 rBV 890591 1893248 100.00% 20.402% 4 25.714 2246 2252 2264 rBV2 819126 1736695 91.73% 18.715% 5 30.332 2752 2755 2760 rVB 9882 19640 1.04% 0.212%

6 30.791 2800 2805 2810 rBV 87493 167804 8.86% 1.808% 7 33.784 3124 3131 3150 rBV2 543583 1299800 68.65% 14.007% 8 38.053 3587 3596 3611 rBV2 336285 1013774 53.55% 10.924%

Sum of corrected areas: 9279886

1797.D GCMS0208.M Thu Feb 28 11:47:28 2002

NYC-WTC_000003749

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NYC-WTC_000003749Source: NYC Law Department, mirrored locally

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