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GCMS blank analysis results, Feb 25-26 2002

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Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.

NYC-WTC_000003425–000003443

Folder label: “GCMS X 1/20/02 A 2/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\0116B.D Vial: 1 . Acq On : 25 Feb 2002 11:14 am Operator: * Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 26 08:18:21 2002 Quant Results File: HP022102.RES

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP020702 Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 9.72 152 1184628 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 5073061 20.00 ug/L 0.00 17) Acenaphthene-diO 18.33 164 2451324 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.63 188 4274830 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 3219213 20.00 ug/L -0.03 44) Perylene-dl2 34.41 264 2203430 20.00 ug/L -0.04

System Monitoring Compounds 37) 2,4-DDD 27.72 235 190006 3.33 ug/L 0.00 Spiked Amount 5.000 Recovery = 66.60% Target Compounds Qvalue 20) Dimethylphthalate 18.33 163 406424 2.73 ug/L + 58 21) 2,6-Dinitrotoluene 18.33 165 315187 9.18 ug/L # 27

(#) = qualifier out of range (m) = manual integration 0116B.D HP022102.M Tue Feb 26 08:18:22 2002 Page 1

NYC-WTC_000003426

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NYC-WTC_000003426Source: NYC Law Department, mirrored locally

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GCMS analysis results, Feb 27 2002 · Box DEP Box 12

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Gas chromatography-mass spectrometry results for sample AE01138 identifying unknown compounds and surrogates on February 27, 2002.

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