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VOCs GC/MS lab blank results, Jan 11 2002

Machine-extracted title · confidence 95%

Gas chromatography mass spectrometry analysis report for a laboratory blank testing volatile organic compounds on January 11, 2002.

NYC-WTC_000003326–000003342

Folder label: “524 1/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02JAN11\0111C10.D Vial: 2 Acq On : 11 Jan 2002 1:15 pm Operator: 206-bh Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 14 9:49 2002 Quant Results File: HP010402.RES

Quant Method : C:\HPCHEM\1\METHODS\HP010402.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Jan 14 09:48:50 2002 Response via : Initial Calibration DataAcq Meth : HP010402

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) CIS-1,3-DICHLOROPROPENE 17.20 75 337876 11.30 ug/L 100 35) TOLUENE 17.97 91 1007920 12.00 ug/L 99 36) TRANS-1,3-DICHLOROPROPENE 18.24 75 286390 11.71 ug/L 99 37) 1,1,2-TRICHLOROETHANE 18.63 97 141262 11.43 ug/L 96 38) TETRACHLOROETHENE 19.40 166 246634 11.86 ug/L 99 39) 1,3-DICHLOROPROPANE 19.14 76 273567 11.55 ug/L 99 40) DIBROMOCHLOROMETHANE 19.82 129 172692 11.33 ug/L 97 41) 1,2-DIBROMOETHANE 20.27 107 123907 11.13 ug/L 97 42) CHLOROBENZENE 21.15 112 669034 11.68 ug/L 100 43) 1,1,1,2-TETRACHLOROETHANE 21.20 131 231252 11.74 ug/L 100 44) 2-HEXANONE 18.53 43 60535 12.36 ug/L 88 45) ETHYLBENZENE 21.20 91 1306608 12.19 ug/L 98 46) P & M-XYLENE 21.36 106 1000393 25.23 ug/L 100 47) O-XYLENE 22.33 91 1109590 12.58 ug/L 98 48) STYRENE 22.40 104 827823 12.44 ug/L 100 49) 1,1,2,2-TETRACHLOROETHANE 23.40 83 193102 12.38 ug/L 96 51) BROMOFORM 23.23 173 103730 10.47 ug/L 97 52) ISOPROPYLBENZENE 23.04 105 1383968 10.75 ug/L 99 53) 1,2,3-TRICHLOROPROPANE 23.72 110 50380 10.04 ug/L 98 54) N-PROPYLBENZENE 23.91 91 1946568 10.86 ug/L 100 55) BROMOBENZENE 24.15 156 332877 10.60 ug/L 91 56) 1,3,5-TRIMETHYLBENZENE 24.24 105 1248802 10.91 ug/L 99 57) 2-CHLOROTOLUENE 24.39 91 1186403 10.58 ug/L 100 58) 4-CHLOROTOLUENE 24.46 91 1182987 10.73 ug/L 100 59) TERT-BUTYLBENZENE 25.02 134 301349 11.50 ug/L 98 60) 1,2,4-TRIMETHYLBENZENE 25.12 105 1391678 11.06 ug/L 99 61) SEC-BUTYLBENZENE 25.48 105 1951004 11.22 ug/L 100 62) P-ISOPROPYLTOLUENE 25.73 119 1558947 11.37 ug/L 99 63) 1,3-DICHLOROBENZENE 26.09 146 816887 10.98 ug/L 98 64) 1,4-DICHLOROBENZENE 26.30 146 803985 10.60 ug/L 99 65) N-BUTYLBENZENE 26.62 91 1710035 11.45 ug/L 100 66) 1,2-DICHLOROBENZENE 27.13 146 725836 11.29 ug/L 99 67) 1,2-DIBROMO-3-CHLOROPROPAN 28.78 157 34882 7.48 ug/L 97 68) NITROBENZENE 28.99 77 254176 216.20 ug/L 98 69) 1,2,4-TRICHLOROBENZENE 30.73 180 431694 11.04 ug/L 99 70) HEXACHLOROBUTADIENE 30.98 225 248132 11.47 ug/L 99 71) NAPHTHALENE 31.41 128 449578 10.40 ug/L 100 72) 1,2,3-TRICHLOROBENZENE 31.95 180 312409 10.57 ug/L 98

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 0111C10.D HP010402.M Fri Jan 25 12:52:37 2002 Page 2

NYC-WTC 000003330

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NYC-WTC_000003330Source: NYC Law Department, mirrored locally

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